Synthesis and characterization of novel metal chelates of 2-(8-quinolinol-5-yl) – methyl amino-5 -phenyl-1, 3, 4-thiadiazole derivatives

Divyesh K Patel1, Kamlesh Chau

Abstract

The Synthesis of novel Metal chelates of 5-Chloromethyl-8-quinolinol coupled with 5-phenyl-(1, 3, 4) thiadiazol-2- ylamine has been carried out in the presence of sodium bicarbonate. The newly synthesised compounds were confirmed on the basis of their spectral characterisation like IR, NMR, Mass and their Elemental analysis. The transition metal chelates viz. Cu2+, Ni2+, Co3+, Mn2+ and Zn2+ of CTAQ were prepared and characterized by metalligand (M:L) ratio, IR and reflectance spectroscopies and magnetic properties