Thermogravimetric analysis of heat treated CR-39 polymer

Renu Gupta, V. Kumar, P.K. Goy

Abstract

Quinazolin-4-one-3-yl-propan-2-one (2) was prepared by N-alkylation of Quinazolin-4(3H)one 1. The treatment of compound 2 with hydrazine hydrate yielded hydrazine derivative (3), which on condensation with variously substituted aryl aldehydes gave the corresponding hydrazones (4). Compound 3 on reaction with phenyl isocyanate and phenyl isothiocyanate transformed into the corresponding carbamates and thiocarbamates (5) respectively. Compound 3 also gave a tricyclic compound (6) when refluxed in presence of ammonium acetate and acetic acid, while hydrazone derivative (7) when treated with dehydroacetic acid.

Relevant Publications in Journal of Chemical and Pharmaceutical Research